A method of head space solid phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry for the determination of tetramethyllead and tetraethyllead in water sample was developed. The conditions of SPME extraction and GC-MS determination were discussed.
The poisoning effects of tetraethyllead (ⅰ) and lead scavengers (ethylene dichloride and ethylene dibromide) on monolithic non-noble metal catalysts have been examined.
对添加了四乙基铅以及扫气剂(二氯乙烷及二溴乙烷)的甲苯对非贵金属燃烧催化剂的中毒情况进行了考察。
The average recoveries of tetramethyllead and tetraethyllead in water were in the range of 87.5%~110.6%.