2, 2-Diethoxypropane was synthesized from acetone and triethyl orthoformate via condensation with acidic cation-exchange resin. The affection to the yield of some factors such as reaction temperature, persistent time, catalyst quantity and reactant ratio were discussed.
摘 要:以酸性阳离子交换树脂为催化剂在无溶剂的条件下,采用丙酮和原甲酸三乙酯缩合来制备丙酮缩二乙醇,通过正交实验和单因素实验得到适宜的反应条件为:反应温度15℃、保温时间10 h、催化剂用量1∶ 80、原料配比n∶ n=1.0 ∶ 1、催化剂用量m∶ m=1 ∶ 100。